Title One-step modification of nano-hydroxyapatite coating on titanium surface by hydrothermal method
Authors Hu, Xixue
Shen, Hong
Cheng, Yan
Xiong, Xiaoling
Wang, Shenguo
Fang, Jing
Wei, Shicheng
Affiliation Peking Univ, Sch Stomatol, Dept Oral & Maxillofacial Surg, Beijing 100081, Peoples R China.
Peking Univ, Acad Adv Interdisciplinary Studies, Ctr Biomed Mat & Tissue Engn, Beijing 100871, Peoples R China.
Chinese Acad Sci, Inst Chem, State Key Lab Polymer Phys & Chem, BNLMS, Beijing 100190, Peoples R China.
Peking Univ, Coll Engn, Beijing 100871, Peoples R China.
Keywords Titanium
Surface modification
Nano-HA
Hydrothermal treatment
Cell affinity
PLASMA-SPRAYED HYDROXYAPATITE
CALCIUM-PHOSPHATE COATINGS
SIMULATED BODY-FLUID
IN-VITRO
LASER DEPOSITION
IMPLANT SURFACES
ION-IMPLANTATION
CELL RESPONSE
PURE TITANIUM
THIN-FILMS
Issue Date 2010
Publisher 表面和涂层技术
Citation SURFACE & COATINGS TECHNOLOGY.2010,205,(7),2000-2006.
Abstract Since metallic biomaterials used for orthopedic and dental implants possess a paucity of reactive functional groups, bioactivity modification of these materials is challenging. To enhance osteoconductivity, sandblasted and acid etched titanium (SIA-Ti) discs were hydrothermally treated in simple suspension of hydroxyapatite (HA) by a one-step method in the present work. Change of surface chemistry, surface morphology of samples, and structure of formed nano-HA were investigated by X-ray photoelectron spectrometry (XPS), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR) and X-ray powder diffraction (XRD). The results demonstrated that the concentration of hydroxyl groups increased after hydrothermal treatment The ability of the titanium surface to form nano-HA was enhanced by increasing the hydrothermal treatment temperature and time. The bonding strength of the formed nano-HA coating, examined by an ultrasonic cleaning process, was higher than that of HA coating generated directly by HA suspension deposition. Culturing of MC3T3-E1 cells on the SLA-Ti and HT-Ti discs in vitro showed that HT-Ti was more favorable for cell attachment and differentiation than SIA-Ti. Hence the one-step hydrothermal treatment with HA suspension was a simple, effective and promising method for HA coating modification of titanium implants. (C) 2010 Elsevier B.V. All rights reserved.
URI http://hdl.handle.net/20.500.11897/154783
ISSN 0257-8972
DOI 10.1016/j.surfcoat.2010.08.088
Indexed SCI(E)
EI
Appears in Collections: 口腔医院
前沿交叉学科研究院
工学院

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